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    Journal of Pharmacology and Pharmacotherapeutics
    Home»Volume 16, Issue 3»Benzoxazinone Derivatives as Antiplatelet: Synthesis, Molecular Docking, and Bleeding Time Evaluation
    Volume 16, Issue 3

    Benzoxazinone Derivatives as Antiplatelet: Synthesis, Molecular Docking, and Bleeding Time Evaluation

    October 10, 20252 Mins Read
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    Kholis Amalia Nofianti1, Juni Ekowati1, Nuzul Wahyuning Diyah1, and Luqmanul Hakim2
    1Department of Pharmaceutical Science, Faculty of Pharmacy, Universitas Airlangga, Surabaya, Indonesia
    2Faculty of Teaching, Universitas PGRI Adi Buana, Surabaya, Indonesia
    Corresponding author(s):
    Kholis Amalia Nofianti, Department of Pharmaceutical Science, Faculty of Pharmacy, Universitas Airlangga, Surabaya 60115, Indonesia. E-mail: kholis-a-n@ff.unair.ac.id
    DOI: 10.1177/0976500X241305440

    Abstract

    Background The recurrence of atherosclerosis is still a global problem. Unfortunately, the drugs currently being used are reported to have resistance. Objectives To prevent the recurrence of atherosclerosis disease, this study developed benzoxazinone derivatives as an antiplatelet agent: 2-phenyl-3,1-benzoxazine-4-one (BZ1) and 2-(4′-chlorophenyl)-3,1-benzoxazin-4-one (BZ2). Materials and Methods The target compounds were synthesized through acyl nucleophilic substitution from acyl chloride and anthranilic acid using a base catalyst in triethylamine. This compound was then given to mice at three different doses to perform bleeding-time and clotting-time tests, using acetosal as a comparison. In silico, the binding energy between the test compound and the cyclooxygenase 1 enzyme was tested using Molegro Virtual Docker version 5.5 (MVD 5.5). The pharmacokinetic parameters were predicted using pharmacokinetics and chemistry through space mapping (pkCSM). Results The synthesis provided 83% yield. The biological assay at a dose of 20 mg/kg body weight (BW) BZ1 showed a higher bleeding time (361 s) than acetosal (324 s), whereas BZ2 was lower (179 s). The molecular analysis revealed that the compound had higher activity than aspirin. The absorption, distribution, metabolism, excretion, and toxicity (ADMET) showed that the compound posed high intestinal absorption. Conclusion This research concluded that both of the synthesized compounds have the potential and prospective to be developed as antiplatelet agents.

    Keywords: Benzoxazinone derivatives, antiplatelet, molecular docking, pharmacokinetics and chemistry through space mapping, cardiovascular disease
    Original Research Article
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